Dissemination of IT for the Promotion of Materials Science (DoITPoMS)

DoITPoMS Micrograph Library Full Record for Micrograph 198

Full Record for Micrograph 198

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Micrograph no
198
Brief description
96% Alumina
Keywords
alumina Link to MATTER Glossary entry for alumina, ceramic Link to MATTER Glossary entry for ceramic, engineering ceramic
Categories
Ceramic
System
Al2O3
Composition
Al2O3 96%, remainder MgO, CaO, SiO2
Standard codes
Reaction
Processing
Fine sub-micron oxide powders such as lime, silica and periclase are mixed with the coarser alumina and fired so they melt and partially react with the alumina forming a liquid phase, which acts to densify the ceramic by capillary action (liquid phase sintering).
Applications
Seals and bearings in corrosive fluid handling systems. Electrical insulation e.g. in fluorescent light tubes.
Sample preparation
Grind and polish. Thermally etch for 10 mins at about 50ºC below sintering temperature.
Technique
Reflected light microscopy
Length bar
250 μm
Further information
The image shows the classic angular shape of corundum (alumina) grains formed in a liquid medium. The intergranular regions are dark and contain the aluminosilicate glass left from the cooled liquid. This liquid will soften at high temperature and limit the maximum use temperature of the ceramic.
Contributor
Prof W E Lee
Organisation
Department of Engineering Materials, University of Sheffield
Date
02/09/02
Licence for re-use
Attribution-NonCommercial-ShareAlike 4.0 International